H. Li; D. Zhao; Y. Cui; C. Dan; S. Ma; L. Wang; J. Liu; Y. Li; Z. Chen; H. Wang
Experimental Mechanics 64 (2024) 1545-1555
Background The size effect and deformation instability exhibited by materials at the micro- and nano-scale constrain the development and application of miniaturized devices. Introducing different defects in materials through different technical means to improve the deformation stability of materials has been the main research point of micro- and nano mechanics.
Objective This paper presents a novel strategy to completely eliminate the instability of microscopic deformations by the introduction of high-density precipitates in aluminum alloys by means of suitable heat treatment.
Methods A suitable heat treatment is used to introduce a high density of precipitates in the 7075 aluminum alloy. Using the Focused Ion Beam technique and in situ micropillar compression tests, micron-sized single-crystal micropillars were fabricated and the size dependence of the strength and strain-hardening behavior of 7075 aluminum alloy was systematically analyzed.
Results Compared with precipitate-free Al–Mg alloy micropillars, the micropillars fabricated from 7075 aluminum alloy exhibited more stable deformation behavior, predominantly due to the impediment of dislocation motion by precipitates. The power-law exponent for yield strength relative to pillar size was determined to approach a near-zero value, indicating a negligible dependency of yield strength on specimen size. Similarly, the smaller the size of micropillar, the higher the hardening rate, which can be rationalized by exhaustion hardening.
Conclusions The proposed method can eliminate the size effect of materials with pillar size above 0.5 μm and leads to a stabilization in deformation behavior. These are advantageous for the application of micro- and nano-sized components in advanced engineering systems.